Separation and purification of squalene from soybean oil
1.. IntroductionIn the refining of soybean oil, most bioactive compounds such as squalene, fatty acid steryl esters (FASEs), tocopherols and free phytosterols are concentrated in intermediate byproducts and waste streams , .SODD is obtained as a byproduct of the deodorization step during the refining of soybean oil.
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Separation and purification of squalene from soybean oil
Separation and purification of squalene from soybean oil deodorizer distillate Article in Separation and Purification Technology 60(2).128-135 · April 2008 with 1,073 Reads DOI. 10.1016/j.seppur
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SEPARATION AND PURIFICATION OF SQUALENE FROM SOYBEAN OIL
SEPARATION AND PURIFICATION OF SQUALENE FROM SOYBEAN OIL DEODORIZER DISTILLATE Author: GUNAWAN, SETIYO ( 1976 03 23 2002 12 1001 ) KASIM, NOVY S YI-HSU JU ABSTRAK. Depending on conditions in the refining process soybean oil deodorizer distillate SODD in Taiwan typically contains about 45 free fatty acids FFAs and 20 triacylglycerols TAGs.
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Separation and purification of squalene from soybean oil
Separation and Purification of Squalene from Soybean Oil Deodorizer Distillate Setiyo Gunawan (古拿旺), Novy S. Kasim (申娜薇) and Yi-Hsu Ju* (朱義旭) Department of Chemical Engineering, National Taiwan University of Science and Technology 台灣科技大學化工系 國科會編號：NSC
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Vegetable Oil Deodorizer Distillate: Characterization
Separation and purification of squalene from soybean oil deodorizer distillate.. Sep. Purif. Technol., 60: 128 – 135. Gunawan, S., Fabian, C. and Ju, Y. H. 2008b. Isolation and purification of fatty acid steryl esters from soybean oil deodorizer distillate.. Ind. Eng. Chem. Res., 47: 7013 – 7018.
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Separation of Nonpolar Lipid from Soybean Oil Deodorizer
In addition, the NPLF contains squalene and FASEs and can be processed further to obtain pure squalene and FASEs as described in our previous work (12 Gunawan , S.. Kasim , N.S.. Ju , Y.H. ( 2008) Separation and purification of squalene from soybean oil deodorizer distillate.
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nents in C. inophyllum seed oil, such as FFA, squalene, TAG, diameter, with a thin, compact, and smooth outer layer, and diacylglycerols (DAG), and monoacylglycerols (MAG) were greyish-green in
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Squalene Extraction: Biological Sources and Extraction Methods
Squalene Extraction: Biological Sources and Extraction Methods ( Vol-2,Issue-4,July - August 2017) Separation and purification stages after extraction can elevate operations cost, one of the most interesting technology to obtain squalene from biological matrix is supercritical fluid extraction with CO2as solvent because of economic, safe
Get PriceMethods for Obtaining and Determination of Squalene from
Another valuable vegetal source of squalene is the soybean oil deodorizer distillate (SODD), a by-product obtained in the deodorization step of soybean oil refining. Being an important oilseed crop, soybean contains 18–20% oil and 40% protein.
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Isolation and Purification of Fatty Acid Steryl Esters
Soybean oil deodorizer distillate (SODD) has been suggested as an alternative to marine animals as a natural source of squalene and a good raw material for the production of fatty acid steryl esters (FASEs), tocopherols, free phytosterols and fatty acids.
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Extraction and Enzymatic Modification of Functional Lipids
squalene in soybean oil deodorizer distillate have been isolated and identified. Separation, purification, and chemical characterization of hydrocarbons fraction in soybean oil
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Optimization of Phytosterols Recovery from Soybean Oil
Gunawan S, Kasim NS, Ju YH (2008) Separation and purification of squalene from soybean oil deodorizer distillate. Sep Purif Technol 60:128–135 CrossRef Google Scholar 5.
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The present invention provides an isolation process of the pure sterols from the SODD by simple acid catalyzed esterification and the separation of the reagents by distillation and water washing followed by the crystallization of phytosterols and purification. Soybean oil deodorizer distillate (SODD) and distillate from other vegetable oil refining contain free sterols, in addition to steryl esters, tocopherols squalene
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Optimization of operating conditions for separation of non
If fresh silica gel is used in modified soxhlet extraction, 100% squalene and 93% FASEs can be removed from SODD and concentrated in NPLF by using a silica gel to SODD mass ratio of
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Factors affecting the content of squalene, total and
One of these, known as Soybean Oil Deodorizer Distillate (SODD), has a potential value in the food and pharmaceutical industries by the presence of compounds with a favorable biological activity such as phytosterols and squalene, the first as hypocholesterolemic agents and squalene as
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Effect of solvent polarity levels on separation of
The aim of this research was to investigate the effect of solvent polarity levels on the separation of xanthone and Kasim N S and Ju Y H 2008 Separation and Purification of squalene from soybean oil deodorizer distillate Separ Purif Tech. 60 128-135. Crossref. Gunawan S, Fabian C and Ju Y H 2008 Isolation and Purification of Fatty Acid
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soybean oil deodorizer distillate
Separation and purification of squalene from soybean oil Depending on conditions in the refining process, soybean oil deodorizer distillate (SODD) in Taiwan typically contains about 45% free fatty acids (FFAs) and 20% triacylglycerols (TAGs).
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Determination of Unsaponifiable Constituents of Deodorizer
Deodorizer distillate is an important by-product obtained during deodorization in the edible oil industries. It is a complex mixture of many health beneficial constituents like phytosterols, tocopherols and squalene. In the present study a simple gas chromatographic method with mass spectrometry was
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Methods for Obtaining and Determination of Squalene from
Extraction of phytosterols, squalene, vitamin E, following the steps (a) Conversion of crude palm oil in palm oil methyl esters (b) 3 short path distillations of PO methyl esters (c) Saponification of phytonutrients obtained in stage (b) (d) Crystallization of phytosterols (e) Solvent partitioning of vitamin E and squalene
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International Journal of Environment, Agriculture and
Separation and purification stages after extraction can elevate operations cost, one of the most interesting technology to obtain squalene from biological matrix is supercritical fluid extraction with CO 2 as solvent because of economic, safe and easy removal characteristics. Keywords—Extraction, Renewable sources, Squalene,
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Free fatty acid separation from vegetable oil deodorizer
free fatty acids from soybean oil deodorizer distillate (SODD) was investigated through molecular distillation, using different operating conditions. Evaporator temperature from 100 to 180 C and feed flow rate in the range of 1.5–23.0 g min−1 were used in the experiments.
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Neutralization of Soybean Oil Deodorizer Distillate for
Soybean oil deodorizer distillate (SODD), a byproduct of the soybean oil refining process, is a complex mixture of compounds, such as free fatty acids (FFA), hydrocarbons, and sterols, such as tocopherols, a class of major natural antioxidants with vitamin E activity.
Get PriceSimulation and thermodynamic modeling of the extraction of
Abstract - Soybean oil is the most consumed vegetable oil in the world, representing 54% of the total world production. Brazil is the second country in the world
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Setiyo Gunawan - Google Scholar Citations
Separation and purification of squalene from soybean oil deodorizer distillate S Gunawan, NS Kasim, YH Ju Separation and Purification Technology 60 (2), 128-135 , 2008
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Simultaneous HPLC–DAD Analysis of Tocopherols
Vegetable oil deodorizer distillates (VODD) are important by-products of deodorization of vegetable oils by high-temperature stripping of volatile components with undesirable flavors. Because valuable components, for example tocopherols, phytosterols, and squalene, are also stripped [1], deodorizer
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Liquid−Liquid Phase Transition of Mixtures Comprising
The favorable separation factors obtained reveal the strength and potential of ethyl lactate as a green solvent for the recovery of squalene from squalene + triglyceride mixtures. Liquid−Liquid Phase Transition of Mixtures Comprising Squalene, Olive Oil, and Ethyl Lactate: Application to Recover Squalene from Oil Deodorizer Distillates
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The deodorizer distillate (or distillate of a vegetable oil deodorization process) can be derived from a soybean oil, a canola oil, a rapeseed oil, a sunflower oil, a rice bran oil, a safflower oil
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